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Author Topic:   Takin' a break
Android
Member
posted 12-23-1999 02:23 AM     Click Here to See the Profile for Android     
My dreamin' sumtimes includes pictures. It looks so real, doesn't it?
Set up a hotbath with a pyrex boiling pot.
1 gram of pure soody was placed in an 8" test tube @ 8:30 pm dreamtiime. Then added 7ml GAA. Temperature was kept on low on the old BettyCrocker hotplate($15 Raley's). After 30 min. or so, 5 drops of H2SO4 was added, test tube was lightly plugged #3, and the heat was turned up to near boiling.
During the next hour and a half, the ACU-RITE (walmart $12.98) showed old Betty was holdin' steady at 97.4 degrees C.
Then I noticed the beautiful clear, watery, homogenized (as UF describes it) was slightly golding up on me, so I stopped dreaming to reflect on the possibles. Unable to EVER not be busy, I decided to post the dream picture of the happy moments before this (whatever, it's only a gram, anyway) curve came up.
Kodak photo GAA. Napa battery acid. H2SO4 listed as only ingredient. Superclean P.E.
I figure battery acid isn't concentrated enough. But I was bored and I got a lifetime of stash so wutdafuk?

CHEMMAN
Member
posted 12-23-1999 04:47 AM     Click Here to See the Profile for CHEMMAN     
Oh shit Dont leave us .Well miss you real badddd

Android
Member
posted 12-23-1999 04:54 AM     Click Here to See the Profile for Android     
Where ya goin', Chemman? I'll miss you, too! Hurry back, though!
Wonder why he wanted to tell me he was leaving? Trying to think of anything I could've said, that would inspire this obvious crush he has on me.
Hope he didn't do anything stupid. Well, anything more stupid than tryin' to flame me that is!

------------------
"ARROGANT & CYNICAL"
(Ticklish,too!)

CHEMMAN
Member
posted 12-23-1999 05:20 AM     Click Here to See the Profile for CHEMMAN     
I aint flamin ya man your OK .A sense of humor is good around here sometimes.Things are bad here at present , buts lets try to keep a

Android
Member
posted 12-23-1999 07:14 AM     Click Here to See the Profile for Android     
How come you're not flaming me? Don't ya like me no more?

Anyway, due to the different color, I decided what it needed was a good bath! What looks like a little wad a gum in there is a stir bar I fashioned to fit in that tiny area. The little mag/stirrer is homemade, too! My stirring hotplate is the size of a television, so too big, bra!
After chargin' it up for 20 min., I poured the solution into the hydrogenator and began stirring. That remindes me, better return to dream and check on that sucka. Would want goldenboy to drown. This method's been around a long time, I know, but it's kinda fun and normally gives ya good microstash.

Android
Member
posted 12-23-1999 08:55 AM     Click Here to See the Profile for Android     
After loggin' 3000 coulombs (And the fact that the steady flow of bubbles mysteriously decided they'd had enough and left without sayin' goodbye 'bout a minute before I stopped the party), I shut 'er down and setup vaccuum filtration using a simple aeriator, 600ml buchner funnel with a porous insert and a single coffee filter(just to keep stains off the porous insert) with a 2L polylab sidearm flask, and poured the reacted (hopefully) solution through just to remove the metallic powder that the silverdollars leave.
Guess I'll go back to the dream and do the last step now. Wish me luck.

Android
Member
posted 12-23-1999 09:49 AM     Click Here to See the Profile for Android     
Poured the clear filtered solution into 1L Sep Funnel. Unfortunately, the phone woke me from the dream. My wife left to go pick her mother at the train station. I'll finish the dream as soon as her mom goes shoppin' er whatever.
I'm always the last one to know in this house!

aqua-girl
Member
posted 12-23-1999 12:08 PM     Click Here to See the Profile for aqua-girl     
Thanks for the Christmas pictures

Whats the power source in this dream? I just can't figure out a good OTC power supply for this electrogizmo stuff. Keep hearing different reports....

Hematite
Member
posted 12-23-1999 12:44 PM     Click Here to See the Profile for Hematite     
Hey did someone forget your maintenance schedule for the likes of disc defragmenting and temp file cleaning etc.?
I ask cause you have to be the slowest and most patient person ever not to be human !!!
The wife left to go to the train station for goodness sake!!!!! I usually get knocked about the head for finding shit like that out tomorroww !
Just finish the damn thing and the hell with this teasing baiting shit ok tinman ?

------------------
Regards,Hematite.


Huffalump
Member
posted 12-23-1999 01:00 PM     Click Here to See the Profile for Huffalump     
Are you saying that you used a silver dollar rather than palladium for the cathode?

Android
Member
posted 12-23-1999 07:36 PM     Click Here to See the Profile for Android     
I'm sorry, but my missuses mum is hovering around like a fruitfly! I feel like I'm trapped in a bad episode of Leave to Beaver.
Huff: I don't have any palladium. Would be nice! Never dedicated any enough time & effort into lectrosynth to find a sources.
Shit! There she is! Later!
Promise! I'm as anxious as you!

Huffalump
Member
posted 12-23-1999 07:48 PM     Click Here to See the Profile for Huffalump     
Complain about a headache, cart everything into the bathroom, and then tell them you're going to take a nice long hot bath until you feel better.

Android
Member
posted 12-23-1999 10:40 PM     Click Here to See the Profile for Android     
Actually, that's a more conservative suggestion than I would expect from you, Huff. Chloroform and duct tape is more Huffianlike.
I did manage to sneak away long enough to neutrallize it, though. I'm out of pre-gassed solvent, so I'll have to wait til dear mum retires to set up a gas generator. Nothing short of an apocalypse will keep me from completing my little dream. I fail to see any significant contribution for anyone outside of entertainment from this, but I've alway been a little naive.
Sweet mum is a couple of feet to my left poring over a crossword puzzle at this very moment whilst I post this.
Wonder what the grieving duration is on accidental mother-n-law terminations?Hmmmmmmmm. Grieving wives are so distracting.

Ain't I a stinker?

------------------
"ARROGANT & CYNICAL"
(Ticklish,too!)

Android
Member
posted 12-23-1999 11:42 PM     Click Here to See the Profile for Android     
Slipped away again and added 100ml of solvent to the base. I chose xylene over toluene mainly because it's been my experience that toluene tends to attract alot of emulsion. Please don't bother to flood me with chemical facts on the two solvents. If you're not happy with the above reason, then just call it "personal preference".
I'm thinking of scrapping the generator for acid drops, what with the present mum situation. It'll fudge the product percentage(if any) calculation, though, since I set aside a portion of the base solvent just in case I go too far on the low side of pH.

Android
Member
posted 12-24-1999 12:06 AM     Click Here to See the Profile for Android     
Oh, aqua girl! Ya never did thank me fer helpin' ya out with your post, but in answer to your question, straight from the battery of my wife's jeep cherokee, baby! I fucked around a few months ago with different power sources and mA DC variators, but an hour of straight 12 from a car battery was the only thing that kept the party going long enough to see results. Probably due my okie old lamp cords and clips from long dead motorcycle battery chargers that keep the amperage around 300DC V mA. But then, I know as little about electronics as I do about chemistry.

Remember: Regardless of real or imagined or dreamed results, this is purely for entertainment purposes only. That's my job at the Hive. Entertainment.(Plus my dreams provide kick-ass go-go for me)

Android
Member
posted 12-24-1999 04:17 AM     Click Here to See the Profile for Android     
With a pH reading that didn't change the pH strip's color,(that's good)I separated the lower layer into a small visionware bowl.
That's a small portable heater on the left, a 60 watt light bulb above right, and it's resting on a heating pad. The piece of paper is for photograghic purposes only. I'm not worried about time at this point. I didn't come this far to be distracted from the hotplate, and have my labor go up in smoke.(Although it does end up in my glass pipe anyway!)
I'll check back soon with the yea or nay. I saved everything, so if this pull produces nothing, I won't bore you with the search which will ensue,(unless ya wanna be) just know that an extensive search will be conducted.

Xtract
Junior Member
posted 12-24-1999 08:55 AM     Click Here to See the Profile for Xtract     
Droid bestus pics ever.......man yo da man ..with youre mom in law there even...can yoiu tell us a little more about da shit ....? would a 15 volt unregulated power source bee OK? What is GAA? And how do you hide all that shit while youre inlaws are a few feet away ??? Yo da man!!!


menotX

aqua-girl
Member
posted 12-24-1999 09:04 AM     Click Here to See the Profile for aqua-girl     
great, thanks. I thought I was gonna have to send you nudie pics of myself to get the answer.

Fuckit, I'll send one anyway ... I used to model for Matrix hair shit ya know!

Mebbe I can whore myself out for precursors... LOL!

Huffalump
Member
posted 12-24-1999 09:58 AM     Click Here to See the Profile for Huffalump     
A picture of Android?

Android
Member
posted 12-24-1999 12:18 PM     Click Here to See the Profile for Android     
I know Xcrement, maybe you should read this again.
aqua girl, you bitch! My computer's cryin' about not being about to read MIME! Shit!
Huff, thank you for post one of my better pics. Handsome devil, aren't I?

Anyhow, awoke this morning after a rare occurence of 'sleep',(think it had something to do with bout of monkey lust with the wife)I found the drying bowl still in a state of evaporation. I was happy to see the layer of almost transparent crystal formation, though. No celebration yet, though. that could be unwashed base salt, or the solution could've flown south on me after checking it's pH. That happens sometimes when doin' the acid drops method.
Hard to photogragh them. Especially after jostling the liquid into them when I moved it for the shot.
Back in a bit with word of the shit.

Android
Member
posted 12-24-1999 01:43 PM     Click Here to See the Profile for Android     
Drying is at last complete!
This thick layer of almost transparent precipitation is all that one would expect from only a gram of starting material. The question now is, is it still just starting material? Or worse, is it one or both of the aforementioned byproducts?
I think a fresh razorblade is now the tool of choice to further investigate this, followed by a wash with a splash of acetone.
I shall return!

dextram
Member
posted 12-24-1999 03:01 PM     Click Here to See the Profile for dextram     
Best of the best there Android, um are them plates in the picture???
Is there any membrane upon them plates.... was/is there any electro film on either of them plates I understand that anodization should free up some of the metal catalyst into the solution this is the metodology, right?
THANKS

very good Mery X-mas to you

Android
Member
posted 12-24-1999 03:18 PM     Click Here to See the Profile for Android     

As for yield, .235gm is less than sad. Most likely a combination of reasons including: my obsessive behavior syndrome with washing the solvent with DH20, the acid drops method of crystalization, the portion I reserved in case I brought the pH too low, inexperience with delicate procedures involved with batches below 1 ounce, inexperience period, etc. That's why I save everything! Because judging by the fact that I am soaring like Fuck Thighlicker just from my unconcious habit of licking the razorblade, the reduction was incredibly successful! What you see before you is a high quality pharmaceutical grade product.
And thus, bringing this entertainment piece to an end. I hope you enjoyed the show. There's gold in them there save jars, and by god, this miner's gonna get busy!
Feel free to ask questions about setup, my sanity, etc. Or just publicly ridicule or flame me! I always enjoy hearing from the Hive membership. I love you all!
Yes, even you, Worlock.

------------------
"ARROGANT & CYNICAL"
(Ticklish,too!)

Huffalump
Member
posted 12-24-1999 05:02 PM     Click Here to See the Profile for Huffalump     
I've got a question:

Is there an indicator that can be used to distinguish between eph and meth? If so, determining if one actually had product could be done before extract & x-tal.

Huffalump

Android
Member
posted 12-24-1999 06:24 PM     Click Here to See the Profile for Android     
That's true, Huff, and there probably is. I'm my only indicator, but I prefer to wait til AFTER crystallization!
This procedure is of not much worth until it can be made large scale at low cost. For me, it's just something to do when I'm in the mood for something to do.
todolu!

CHEMMAN
Member
posted 12-24-1999 07:31 PM     Click Here to See the Profile for CHEMMAN     
Very nice pics.Very entertaining.Yes I find the consumption method the best indicator.
Test it a few times to be sure
Happy Xmas

mrr pyrex
Member
posted 12-24-1999 09:12 PM     Click Here to See the Profile for mrr pyrex     
Well from the appearance, I can say without ANY doubt andriod that was as pure as pure gets. I have seen mixtures, and mixtures will leave those nasty pinwheel lookin creations. When you get plates like that, well I be willing to bet Andriod is spinnin like a 78 record, unless andriods get spun from E and not Meth ;-) Me not knowing andriods physiology(sp?) and all. But regarding telling the difference there is Marquis Reagent and it does give definte results---Orange is E or Pfed//Brown to darkening brown/black is Meth. If it stays orange your SOL, otherwise your doing somethin right. Pyrex clause
P.S.-nice write up driod

mrr pyrex
Member
posted 12-24-1999 09:31 PM     Click Here to See the Profile for mrr pyrex     
Huffy, took me three times of rollin past it before I saw it but HOLY FUC*ING SHI*....RRRRRROOOOOFFFFLLLLL!! gessss those blinkin eyesss bbbhaaawwaaaa

Huffalump
Member
posted 12-24-1999 10:20 PM     Click Here to See the Profile for Huffalump     
I've got a friend, and he's thinking:

Low yeilds aside, I think this is the method for me. I've got 72g of clean pfed and have been waiting for an opportunity to dispose of it... dispose meaning that I no longer have any pfed, whatever it may become. I was going to use iodine and rp, but a recent post here made me a bit nervous, and I also feel very wary about ordering any pyrochem right now because of the general insanity surrounding the millenium. I was going to do electro, but Pd isn't cheap, and although I'm not fundless, the $405 (a coin, not an ingot) I was quoted would take quite a chunk out of my playtime. As things are, I don't sell drugs, and although I still use them quite a bit(more than I'd like), they aren't so much of a lifestyle. I work for my money now, which ain't bad (even if it does suck), but there's no quick money schemes like there used to be... so saving is slow. But, back to the point, I did consider using silver, and was going to try it out, silver being a noble metal and all... and no, I never searched to see if it would work. I'm rambling a little bit, but let me just say that this thread is inspiring. Using silver rather than Pd--not to mention the low overhead and scavenge-a-bility of all the other equipment--really puts this in my right-about-now range. And, since I don't plan on selling any of it, I really don't care about yeilds anyways... which probably wouldn't be too great for a first time methsynth no matter what path I chose to take.

That's what he said, that crazy drunk fuck, I've got no affiliation with him whatsoever. Nice work Android,

Huffalump

Huffalump
Member
posted 12-24-1999 10:29 PM     Click Here to See the Profile for Huffalump     
Two more questions:

1. Did you get your wife a digital camera for christmas? The turnover and candidness of those photos makes me wonder.

2. You had monkey-sex with your wife while her mother was in the house? You're one sick bitch.

Huffalump

dextram
Member
posted 12-24-1999 11:57 PM     Click Here to See the Profile for dextram     
I gues homade from nicle plate and stuff from coins ans a plate if need be of not CO but lead Co in the glaze old blue plate, this lead patr of the gizmo is hooded with a gas extraction port and likewise not shown the hydrogen is bubbled inthrough to cause addational hydrogenation and catalytic activity upon the electrode of interest I like that little nudge at the bottom, tell us more??? Is a tiny amount of quantitary mathyamine added to get things going or have ya siply follwed directions?

dextram
Member
posted 12-25-1999 12:13 AM     Click Here to See the Profile for dextram     
second gueese the picture is of an ashtray of covered in some kinda membrane it looks though like a speaker? It is a lead glazed Cobalt colored ashtray with a protective covering prally with attacjed a spread array of multiple attaching small wire leads from the bundel ussing most proally some kinda lead soder? possibly a rubber glove? the other one looks like it is a doual pound silver dollar assortment

dextram
Member
posted 12-25-1999 12:16 AM     Click Here to See the Profile for dextram     
pantyhose humm interesting methodology

dextram
Member
posted 12-25-1999 12:19 AM     Click Here to See the Profile for dextram     
I bet you drink alot of coffe? more than any normal consumer.

Android
Member
posted 12-25-1999 01:22 AM     Click Here to See the Profile for Android     
If you're finished, Dex, I'd like to squeeze in here for a brief chat with Huff.
Huff:
Make sure you do the research. I don't want to be responsible for any failures or loses of supplies you or any other member might suffer. One of the main reasons I stress that this dream pictorial is for entertainment purposes only.
Now, if you pursue this for your own reasons only, then I wish you great success!
To the others:
There are two silver dollars. The flattened out one visible, and the one that's tucked neatly into a same-shaped piece of pottery.(It's a lid off one of those decorative little candles which I swiped from my wife's knick-knack shelf) A lid from a bottle of H2SO4 snaps perfectly into the back of it after inserting the coin. A tiny hole was drilled in the coin to attach the wire. A tiny hole was drilled into the lid to allow for the wire. Near this hole, a larger hole was drilled for filler port.(for the acid/water mix) This, of course, is the top, and kept above the level of acid/water in the main chamber.
Some of the questions must be translated from chem-jargonese. I'm happy to say, I speak common-man American only.

dextram
Member
posted 12-25-1999 03:23 AM     Click Here to See the Profile for dextram     
My eyes are burning but yes I will bemoth back to my lair for a while it seems.....

mrr pyrex
Member
posted 12-25-1999 03:35 AM     Click Here to See the Profile for mrr pyrex     
GAA=Glacial Acetic Acid Pyrex out

chencho
Member
posted 12-25-1999 01:16 PM     Click Here to See the Profile for chencho     
Android,
Well I guess this pretty much supports the opinion that pfed works as well as ephed. Thanks for sharing.

Android
Member
posted 12-25-1999 02:41 PM     Click Here to See the Profile for Android     
Clencho:
But of course!

Huff. I have an old G.E. full-size camcorder. I also have Snappy software installed on my computer. Between the two. . well, you see the results.
Isn't this thread testiment enough to my being sick? In fact, I'm crazy to the point sanity! Kinda like drinkin' yerself sober.

My writing skills are about the only thing I retained from college. They're weak, at best. Oh, yeah, liver damage. Can't get through college without liver damage.

Merry Christmas!

------------------
"ARROGANT & CYNICAL"
(Ticklish,too!)

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